Publications Scientifiques

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    FTIR analysis and rheological behavior of bisphenol : a diglycidyl ether resin filled Fume-Silica
    (2014) Irekti, Amar; Bezzazi, Boudjema; Boualam, Chahrazed; Aribi, Chouaib; Dilmi, Hamid
    Silica-fume as fillers into polymers materials affect significantly the physical, mechanical and the electrical properties of the polymers. The polymer that we studied here is an epoxy based resin (STR) and silica fume (FS). This paper presents the dependency of the rheological behavior of the STR epoxy resin on the FS content within a temperature at which the reaction thermoset is neglected. We used a cone-plate viscometer for the study of the rheological behavior, and a scanning electron microscope is used for the analysis of the dispersion state of the FS in STR epoxy resin. Compared to the control without loads, an increase of 50% of the shear stress and the plastic viscosity were recorded for the composite. The software Rheowine viscometer enabled us to model and identified the rheological behavior of these mixtures with resin. The results obtained in this modeling, confirmed that the resin mixtures have shear-thinning rheological behavior, this last give us the model of Ostwald de Waele
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    Rheological study of composite materials based on thermosetting matrix and fillers mineral
    (2013) Irekti, Amar; Bezzazi, B.
    In the development of composites materials, the matrix acts as a binder of different reinforcements can distribute the stress, provide good resistance to chemical structure and the desired shape to the final product. But there are still some drawbacks that arise in the physicochemical and mechanical properties of thermosetting matrices. Our job is to synthesize composite materials with news formulations of thermosetting matrices (Granitex products) by the incorporation of 40% of local mineral fillers. The latter give the matrix properties which it does not have, first, to reduce the cost of composite materials, and secondly, to improve implementation by increasing the viscosity and reducing the withdrawal to its minimum value. Rheological testing of mixtures prepared is made on the cone-plate viscometer, or the sample undergoes a shear in the conical space between the plane and the cone. The geometry of the cone - package ensures constant velocity gradient throughout the volume. The rheograms obtained, represents the evolution of the shear stress as a function of shear rate of resin mixtures containing 35% of mineral filler (pozzolan). The mineral filler increases significantly in rheological parameters, whatever the nature of the mineral filler. Compared to the control without charges, an increase of 60% of the shear stress and that of plastic viscosity were recorded for the epoxy resin. The software Rheowine viscometer, enabled us to model and identified the rheological behavior of these mixed with resin. The results obtained in this modeling, confirmed that the resin mixtures have shear-thinning rheological behavior and their behavior follows the model of the Ostwald of Waele
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    Rheological behavior of the epoxy resin loaded with the pozzolan
    (2012) Irekti, Amar; Hami, Brahim; Aribi, C.; Bezzazi, B.; Briki, I.
    The study is to synthesize composite materials with news formul ations of thermosetting matrices by the incorporation of 40% of mineral fillers to reduce the cost of composite materials an d to improve implementation by increasing the viscosity and redu cing the withdrawal to its minimum value. The mineral filler increases si gnificantly in rheological parameters, whatever it nature of th e mineral filler. Compared to the control without charges, an increase of 60% of the shear stress and that of plastic viscosity were reco rded for the epoxy resin. The software Rheowine viscometer enabled us to m odel and identified the rheological behavior of these mixtures wit h resin. The results obtained in this modeling, confirmed that th e resin mixtures have shear-thinn ing rheological behavior, this last allows the model of the Ostwald de Waele