Publications Scientifiques

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    Efficiency Evaluation of Anti-corrosion Treatment of Carbon Steel by Extracts of Red Algae Collected from Mediterranean Coast
    (Revista de Chimie SRL, 2021) Khoukhi, Faiza; Kebbouche-Gana, Salima; Djelali, Nacer Eddine; Gana, Mohamed Lamine
    The paper presents the assessment of inhibition effectiveness of biomolecules extracted from red seaweed against biocorrosion in the petroleum industry. The first objective of this study was to obtain extracts (A, B and C, prepared respectively from red algae species: Corallina ellongata, Gymnogongrus crenulatus and Pterocladia capillacea) by ethanol extraction method. The infrared spectra of the three extracts confirmed the presence of amine derivatives molecules known by their anti-corrosion inhibiting powers. The second objective was based on the identification of physico-chemical characteristics of the extracts and thus revealing their inhibitory and / or bactericidal power in bacterial corrosion of carbon steel in injection water contaminated with sulfato-reducing bacteria. Biological test of all extracts gave a concentration upto 10 germs/mL in contaminated water by sulfato-reducing bacteria during 28 days of incubation at 37°C. Evolution in time of the open-circuit potential showed a longer incubation time for electrolyte with extracts, whereas the stabilization time was shorter. Current corrosion density, polarization resistance, charge transfer resistance and double layer capacity were determined by using linear polarizarion resistance technique and electrochemical impedance spectroscopy. The corrosion protection efficiency of extract obtained from Gymnogongrus crenulatus (extract B) reached a maximum protective capacity of 99.69% at 5 ppm in the injection water.
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    The Application of Enzymological Techniques for Determination of the Inhibitor Activity of Bio Enzym Extracted from Seawater Bacteria P s eudomonas aerogenosa to Fight Biocorrosion of Carbon steel
    (Central de Documentare Al Industriei Chimice Ri, 2017) Khoukhi, Faiza; Kebouche, Salima; Djelali, Nacer-Eddine; Gana, Mohamed Lamine
    The paper presents a studies for the development of new corrosion inhibitors by biotechnological way applicable to many areas of petroleum industry including, characterization of protective films on carbon steel and biocorrosion inhibition. Our research is oriented towards the isolation of new strains of bacteria from the sea waters of the Mediterranean region that have power (inhibitory and/or bactericidal that blocks the growth of sulfate-reducing bacteria responsible for microbiologically influenced by production of Pyocyanin (1 hydroxyphenazin) or 5-methylphenazin-1-one. Our first objective was to isolate the population of Pseudomonas Aerugenosa on a specific medium, characterization gram, then fermentation in a nutrient broth. The second objective of this study is evaluation of corrosion rate by weight loss method with injecting different dose of the crude enzyme extract CEE containing the methylphenazine (Pyocyanin). An efficacy test was performed on test kit vials containing the specific culture medium with the SRB contaminated with industrial injection water from SONAHESS region. The total disappearance of the SRB is 40% of CEE by blocking their metabolism in the growth phase confirms the efficiency of treatment
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    Analyze and modelingofdamage behavior of a C0.12%Mn1.02%Si0.29% HLE steel solicited in selected physicochemical medium
    (Mohammed Premier University, 2015) Belahcene, B.; Benmoussat, A.; Mansri, A.; Doghmane, Mohamed Zinelabidine
    The influence of environment and physical parameters on C0.12%Mn1.02%Si0.29% HLE steel steel corrosion damage behaviour in NaCl solutions was studied using weight loss, pH evolution at 300k to 370k, electro-exchanges, and passivity. Herein, the results show that the corrosion rate changes versus type of thermal treatment and cooling fluid, solution concentration, shape, size and cooling speed of the samples. The resolution of Nernst equation proves that the increase in temperature has a direct effect on hydrogen potential of the solution, current and corrosion potential of the metal. Moreover, the inhibition efficiency was determined by theoretical calculation using mechanical molecular and semi-empirical method. These results guided us to conclude that the inhibitor, which has low electronegativity than C0.12%Mn1.02%Si0.29% Steel has good efficiency
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    Shale problems and water-based drilling fluid optimisation in the Hassi Messaoud Algerian oil field
    (2010) Khodja, Mohamed; Canselier, Jean Paul; Bergaya, Faiza; Fourar, Karim; Benmounah, M. Abdelbaki
    Drilling fluid formulation and properties play a fundamental role in drilling operations. Clay minerals behave initially as a beneficial rheological adjuvant in drilling muds. Nevertheless, the contamination of oil reservoirs by clay minerals present in the drilled geological formation (shales) may generate major problems during drilling as plug formation. In this context, our study deals with the optimisation of drilling conditions in the Hassi Messaoud Algerian field. The mineralogical heterogeneity of this field is first discussed. The rheological and filtration characteristics of water-based muds with different polymer and electrolyte concentrations are investigated. The physical and chemical changes of both drilled formation and drilling fluid during the drilling process are studied. Therefore, depending on the clay present in the geological formation, an optimised drilling fluid system using a new filtration procedure is proposed. A good correlation is found between filtration/rheological properties and inhibition