Browsing by Author "Lecomte-Nana, G."

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    Sintering and final properties of kaolinite-magnesite tapes for the manufacture of cordierite-mullite ceramics
    (Blackwell Publishing, 2020) Hammas, Aghiles; Lecomte-Nana, G.; Daou, Imane; Zibouche, Fatima
    The present work aims at studying the effect of the sintering temperature and magnesite addition on the structure and final properties of silicate ceramics tapes. A kaolinitic clay from Algeria was selected and mixed with different magnesite contents (≤12 mass%). Tape casting process was used to produce the green tapes in an aqueous system with optimized amount of surfactants. The green tapes were fired from 1000°C to 1200°C using a dwelling time of 30 minutes. The effect of the dwelling time was investigated for a firing temperature of 1200°C namely: 30 minutes, 1 hour 30 minutes and 3 hours for samples with 6 and 12 mass% of magnesite. Regarding firing conditions, crystalline phases, thermal conductivity, porosity, and flexural strength were analyzed. The results showed that increasing the sintering temperature to 1200°C tended to significantly decrease the total porosity of samples, which led to the improvement of the stress to rupture values. Specimens with 6 and 12 mass% sintered during 3 hours exhibited highest stress to rupture values (≈117 MPa) and lowest thermal conductivity (<0.2 W.m−1.K−1) and moderate open porosity (27%). The as-obtained ceramics appeared promising for further utilization in refractory industry, thanks to the presence of both cordierite and mullite phases