Publications Internationales

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Author: search.filters.author.Jawaid, Mohammad

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    Physical, mechanical and thermal properties of Spanish broom (Spartium junceum L.) fibre reinforced unidirectional polyester composites
    (SAGE, 2025) Djerad, Abdelkader; Benhamadouche, Lamia; Moussaoui, Nafissa; Bennouioua, Tahar; Jawaid, Mohammad
    This research analyses Spanish broom fibres (Spartium junceum L.) as possible reinforcement in polymer composites. It includes fibre extraction, characterisation, and composite construction. We extracted the Spanish broom fibres by water retting for 30 days, followed by hand washing and air drying. The fibres were spun into skeins using circular spinning. The fibres exhibited a density of 1.27 ± 0.03 g/cm3 and an average diameter of 170 ± 1.80 μm. The SEM investigation revealed a rough, uneven surface with microfibrils and spaces, that are typical of lignocellulosic fibres. Cellulose, hemicellulose, and lignin were detected using FTIR analysis. TGA revealed three weight-reduction phases, with the most significant cellulose degradation temperature around 319°C. XRD analysis revealed a 48.09% crystallinity index and 15.7 nm crystallite size. Single fibre tensile testing showed an elastic modulus of 20.51 ± 5.30 GPa, a fracture stress of 486.17 ± 129.16 MPa, and a fracture strain of 1.57 ± 0.43%. Spanish broom yarn and polyester resin were used to create unidirectional composites. Results indicate that both unreinforced polyester and SJL fibre-reinforced composites have enhanced mechanical characteristics, with maximum stress of 29.79 ± 0.79 MPa and Young’s modulus of 3.10 ± 0.25 GPa. This work highlights the significance of employing Spanish broom fibres as a green reinforcing material for polymer composites and suggests future research options
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    Exploring tensile properties of bio composites reinforced date palm fibers using experimental and Modelling Approaches
    (Elsevier, 2024) Saada, Khalissa; Zaoui, Moussa; Amroune, Salah; Benyettou, Riyadh; Hechaichi, Amina; Jawaid, Mohammad; Hashem, Mohamed Ibrahim; Uddin, Imran
    The objective of this study was to assess the tensile strength of epoxy bio-composites reinforced with palm fibers, both untreated and treated with sodium carbonate NaHCO3 at a concentration of 10 % (w/v) for 24 and 96 h, with varying weight percentages of fibers (15 %, 20 %, 25 %, and 30 %). To predict the mechanical performance of the composites, two methods were employed: artificial neural network (ANN) and response surface methodology (RSM). A Box-Behnken RSM design was used to conduct experiments and establish a mathematical model of the bio-composite behavior as a function of the fiber percentage in the samples, specimen cross-section, and treatment time. The ANN forecasts showed consistent expected values for the bio-composite sample behavior, with a correlation coefficient (R2) greater than 0.98 for Young's modulus and 0.97 for stress. Similarly, the correlation coefficients obtained by RSM for the mechanical properties were also highly satisfactory, with an R2 of 0.89 for Young's modulus and 0.87 for stress. Finally, the errors generated by each method (Box-Behnken and ANN) were compared to the experimental results.
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    Nanocrystalline cellulose from microcrystalline cellulose of date palm fibers as a promising candidate for bio-nanocomposites : isolation and characterization
    (MDPI, 2021) Hachaichi, Amina; Kouini, Benalia; Kian, Lau Kia; Asim, Mohammad; Fouad, Hassan; Jawaid, Mohammad; Sain, Mohini
    Date palm fiber (Phoenix dactylifera L.) is a natural biopolymer rich in lignocellulosic components. Its high cellulose content lends them to the extraction of tiny particles like microcrystalline cellulose (MCC) and nanocrystalline cellulose (NCC). These cellulose-derived small size particles can be used as an alternative biomaterial in wide fields of application due to their renewability and sustainability. In the present work, NCC (A) and NCC (B) were isolated from date palm MCC at 60 min and 90 min hydrolysis times, respectively. The isolated NCC product was subjected to characterization to study their properties differences. With the hydrolysis treatment, the yields of produced NCC could be attained at between 22% and 25%. The infrared-ray functional analysis also revealed the isolated NCC possessed a highly exposed cellulose compartment with minimized lignoresidues of lignin and hemicellulose. From morphology evaluation, the nanoparticles’ size was decreased gradually from NCC (A) (7.51 nm width, 139.91 nm length) to NCC (B) (4.34 nm width, 111.51 nm length) as a result of fragmentation into cellulose fibrils. The crystallinity index was found increasing from NCC (A) to NCC (B). With 90 min hydrolysis time, NCC (B) showed the highest crystallinity index of 71% due to its great cellulose rigidity. For thermal analysis, NCC (B) also exhibited stable heat resistance, in associating with its highly crystalline cellulose structure. In conclusion, the NCC isolated from date palm MCC would be a promising biomaterial for various applications such as biomedical and food packaging applications
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    Extraction and characterization of microcrystalline cellulose from date palm fibers using successive chemical treatments
    (Springer, 2021) Hachaichi, Amina; Kouini, Benalia; Kian, Lau Kia; Asim, Mohammad; Jawaid, Mohammad