Publications Internationales

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    Bacterial Population Kinetics and Physicochemical Profiles in Fermented Goat Milks: Roles of Streptococcus thermophiles ATCC19258 and Lactobacillus bulgaricus ATCC11842
    (National Nutrition and Food Technology Research Institute, 2025) Tayeb, Silarbi; Morsli, Amirouche; Saadia, Laabas; Mohamed, Chahbar; Khaled, Hamden; ben Salah-Abbes, Jalila
    Background and Objective: The fermentation of Algerian goat milk, a process for the production of valuable dairy products, relies on the synergistic activity of Streptococcus (S.) thermophilus and Lactobacillus (L.) bulgaricus. However, a significant knowledge gap is seen regarding the precise dynamics of these starter cultures within the unique matrix of Algerian goat milks. Specifically, the intricate relationships between their growth patterns and the resulting physicochemical changes, which regulate the distinct biochemical characteristics of fermented products, are poorly understood. So, this study addressed this problem by studying specific contributions of S. thermophilus and L. bulgaricus to goat milk fermentation. Material and Methods: Goat milk was fermented by starter cultures of S. thermophilus and L. bulgaricus (8 h). Bacterial growth and physicochemical parameters, including pH, titratable acidity, viscosity and syneresis, were assessed. Mixed-effects models were used for statistical analysis to assess the relationship between physicochemical changes and bacterial growth. Results and Conclusion: The results showed a strong relationship between L. bulgaricus and the control of acidification, viscosity and syneresis (r = 0.979 for titratable acidity, p < 0.0001). S. thermophilus contributed significantly, particularly to the increases in viscosity (r = 0.773, p < 0.01). The two species significantly decreased the pH, with L. bulgaricus having twice the acidifying effects. By the end of the fermentation process, pH reached 4.12 ±0.20, titratable acidity increased to 84.75 ±2.19 °D and viscosity increased to 6425.00 mPa.s ±638.64. The final bacterial counts of S. thermophilus and L. bulgaricus were 519.00 ±115.29×10⁷ and 65.54±6.89×10⁷ CFU.ml-1, respect-ively. In addition to providing a robust statistical framework for process control and quality assurance in fermented milk manufacture, this study highlighted the critical role of L. bulgaricus in regulating structural and sensory qualities of fermented goat milks. Results can be used to optimize fermentation processes for goat milk by strategically manipulating the ratio of L. bulgaricus to S. thermophilus. The strong correlation between L. bulgaricus and acidification, viscosity and syneresis (r = 0.979 for titratable acidity, p<0.0001) provides a clear target for controlling key product attributes
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    Maximizing enhanced oil recovery via oxidative cracking of crude oil: employing air injection and H2O2 with response surface methodology optimization
    (IOP publishing, 2024) Nouari, Omar; Hammadou née Mesdour, Souad; Boudjemaa, Hamada
    The utilization of air injection as a method to enhance oil recovery in oil fields has gained prominence due to its cost-effectiveness and widespread availability, particularly in heavy oil production. This study focuses on optimizing the oxidative cracking process of Algerian crude oil by employing air injection supplemented with H2O2 and analyzing the interaction of key operating parameters like temperature and catalyst amount using response surface methodology. The predicted values derived from the response functions closely aligned with experimental data, demonstrating high accuracy (R2= 0.9727 for liquid oil, R2= 0.9176 for residue, and R2= 0.7399 for gas phases). Using the developed second-order model, optimal conditions were determined through contour and surface plots, as well as regression equation analysis using Design software. At these optimal parameters (14.78 wt% of H2O2, 2 l min−1 of air flow, 100 ml of crude oil at 354.05 °C for 40 min), the oxidative cracking process yielded 96.32% liquid oil, 3.018% residue, and 0.662% gas products. Notably, the experimental produced liquid oil constituted 96.07 vol. %, matching well with the optimization outcomes. Physicochemical analysis of liquid product phase obtained from oxidative cracking process of petroleum confirmed the prevalence of light aliphatic compounds(C2-C11) at 70.59%, alongside 29.41% of C12-C36. The process also resulted in reduced viscosity, density, refractive index, and sulfur content in the liquid phase. The combination of air injection and H2O2 showcases promise in recovering residual oil effectively and contributes to the ongoing advancements in EOR techniques.
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    RHEOLOGICAL AND MECHANICAL BEHAVIOR STUDY OF ECO-FRIENDLY CEMENT MORTAR MADE WITH MARBLE POWDER
    (University of Zielona Gora, 2024) Chahour, Kahina; Mechakra, Hamza; Safi, Brahim; Dehbi, Nacera-Melissa; Chaibet, Cylia
    The work aim is to investigate the rheological and mechanical behavior of an eco-friendly mortar made with marble powder. Marble is have used as sand (total substitution of natural sand) and as an additional material (partial substitution of cement). Firstly, rheological tests were carried out on the cement pastes in order to study the effect of cement substitution by marble powder on the rheological behavior. Secondly, our study is devoted to evaluate the mechanical performances (flexural strength, compressive strength, mechanical behavior and ultrasonic pulse velocity) of a fluid mortar such as the case of the self-compacting mortars elaborated with the marble powder as an addition a material and as sand. The mechanical test results show that compressive strength and mechanical behavior of an ecological cement mortar made with marble waste as natural sand improved significantly. However, marble-based mortars with 100% of marble sand have given a mechanical strength similar to that obtained by control cement mortar (100% natural sand). It was also noted that it an ecological cement mortar made with 30% of marble powder as an addition a supplementary material can be obtained. This leads to a reduction in cement consumption and a reduction in CO2 gas emissions caused by cement production.
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    Rheological behavior and microstructural properties of crude oil and emulsions (water/oil-oil/water)
    (Taylor & Francis, 2024) Yacine, Celia; Safri, Abdelhamid; Djemiat, Djamal Eddine; Benmounah, Abdelbaki
    An experimental study on crude oil (from the Tin Fouye Tabankort oil field in southern Algeria) was carried out. This study allowed us to understand the rheological behavior of this crude oil with these different emulsions and how it reacts under the effects of temperature and the inversion of its phase from E/H to H/E. So we measured the rheological characteristics by tests flow and dynamic mode at different temperatures from 10 °C to 50 °C and at different water concentrations (20.40.50.60 and 70%) at a fixed temperature of 20 °C. The increase in temperature results in a 31.84% reduction in the initial viscosity of the crude oil. The addition of the volumic fractions of water results in an increase in viscosity at the point of inverse, which will decrease the apparent viscosity of these emulsions where the emulsions (W/O) come from (O/W). This crude oil and their emulsions exhibit a non-Newtonian behavior with shear thinning. The dynamic analysis depends on the temperature and the percentages of water added to the crude oil. At the end, a microscopic analysis was added to verify the relationship between the shape and diameter of the water droplets in each emulsion and the viscosity variation.
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    An ecological water‑based drilling mud (WBM) with low cost: substitution of polymers by wood wastes
    (Springer, 2019) Haider, Soumia; Messaoud‑Boureghda, Mohamed‑Zine; Aknouche, Hamid; Akkouche, Ali; Hammadi, Larbi; Safi, Brahim
    An ecologically friendly water-based drilling mud (WBM) was designed by using wood wastes (WP: wood powder) in order to substitute the organic polymers which are very expensive and often make the higher cost of the oil well drilling. This present work is dedicated on studying the rheological behavior and main rheological properties of WBM containing the wood powder at different contents and sizes by substitution of usually used polymers. The effect of wood powder on the drilling fluid filtrate was also analyzed. The drilling fluid that was developed has better rheological properties and fluid loss control which are required for a good functioning of oil well drilling. By a total substitution of polymers, the wood powder (300 μm at 850 kg/m3) can be used as a filtrate reducer of mud because the WBM filtrate obtained exhibits a minimum and having requested values for such formation
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    Rheological behavior of oil sludge from Algerian refinery storage tanks
    (Elsevier, 2022) Souas, Farid
    Rheological behavior of oil sludge from Algerian refinery storage tanks Farid Souas a, b, * a LEGHYD Laboratory, Faculty of Civil Engineering, University of Science and Technology Houari Boumediene (USTHB), Bab Ezzouar, Alger, Algeria b Research Unit Materials, Processes and Environment (UR-MPE), Faculty of Engineering Science, University M’Hamed Bougara, Boumerdes, Algeria a r t i c l e i n f o Article history: Received 15 August 2021 Received in revised form 20 December 2021 Accepted 28 January 2022 Available online xxx Keywords: Crude oil Rheology Sludge Storage tank Temperature Viscosity a b s t r a c t The consumption and demand for petroleum are increasing dramatically with the rapid development of industry and energy sector. As a result, petroleum refineries produce the greatest amount of oily sludge formed at the bottom of storage tanks during oil storage operations, which has a severely negative impact on the storage capacity and the operational safety of the storage tank. The present study focuses on the rheology of this complex fluid from Algerian crude oil storage tanks. Rheological measurements were performed at different temperatures under steady shear and dynamic oscillometry using AR-2000 Rheometer. The results obtained show that the sludge exhibits yield-pseudoplastic flow behavior at low shear rates, which is adequately described by the Herschel Bulkley model based on the standard error and correlation coefficient values. However, quasi-Newtonian flow behavior occurs at very high shear rates. The increase in temperature had positive effects on the rheological properties of the sludge, including dynamic viscosity, shear stress, yield stress, complex modulus, elastic modulus and viscous modulus. The dynamic rheology studies have shown that the sludge material behaves more like a solid than a liquid under all experimental conditions studied
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    Rheological behavior of cement-based grout with Algerian bentonite
    (Springer Nature, 2019) Benyounes, Khaled
    he rheological parameters, yield stress, flow index, consistency, and plastic viscosity of cement grouts are important parameters for the quality control of these materials. These parameters are assessed from the rheogram using a rheo-logical model. Cement slurries without additive indicated a non-Newtonian type of rheological behaviour with yield stress. On the other hand, the mixtures containing a viscosifying agent exhibit a shear-thinning rheological behaviour which is much more important than the mixtures without a viscosifying agent. In this work, we formulated non-hydrated Algerian bentonite cement slurry in the presence of a superplasticizer. Cement was replaced cement by bentonite in five different substitution rates (2%, 4%, 6%, 8%, and 10%) and the water/binder ratio was fixed at 0.5. For this, various rheological tests were realized by using a controlled stress rheometer. In order to show the influence of bentonite on the rheological behaviour of the different grouts, several flow tests were carried out for a range of shear rates between 0.01 and 200 s−1. To properly adjust the different rheograms, various rheological models were used such as the models of Bingham, Herschel–Bulkley, modified Bingham, Casson, De Kee, Vom Berg, Yahia and Papanastasiou. For the correct choice of the rheological model, it was based on the calculation of the standard error. It was found that the rheological models of Herschel–Bulkley and Papanastasiou made it possible to better describe the flow curves compared to the other rheological models. It has been found that as the content of bentonite increases, the yield stress and the consistency evolve drastically, by cons the flow index decreases progressively
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    Modeling viscosity of CO 2 at high temperature and pressure conditions
    (Elsevier, 2020) Nait Amar, Menad; Ghriga, Mohammed Abdelfetah; Ouaer, Hocine; Ben Seghier, Mohamed El Amine; Thai Pham, Binh
    The present work aims at applying Machine Learning approaches to predict CO2 viscosity at different thermodynamical conditions. Various data-driven techniques including multilayer perceptron (MLP), gene expression programming (GEP) and group method of data handling (GMDH) were implemented using 1124 experimental points covering temperature from 220 to 673 K and pressure from 0.1 to 7960 MPa. Viscosity was modelled as function of temperature and density measured at the stated conditions. Four backpropagation-based techniques were considered in the MLP training phase; Levenberg-Marquardt (LM), bayesian regularization (BR), scaled conjugate gradient (SCG) and resilient backpropagation (RB). MLP-LM was the most fit of the proposed models with an overall root mean square error (RMSE) of 0.0012 mPa s and coefficient of determination (R2) of 0.9999. A comparison showed that our MLP-LM model outperformed the best preexisting Machine Learning CO2 viscosity models, and that our GEP correlation was superior to preexisting explicit correlations.
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    A review on the rheology of heavy crude oil for pipeline transportation
    (ELSEVIER, 2020) Souas, Farid; Safri, Abdelhamid; Benmounah, Abdelbaki
    Given the combination of rising global energy demand and the decline in conventional crudes, heavy crudes are generally considered to be the future energy resource. In many regions of the world, heavy crude oil must be transported through pipelines from the point of production to storage facilities or refineries. The transportation of heavy crude oil by pipeline poses serious problems related to the high viscosity and flow difficulties, particularly in cold climates or offshore conditions. Indeed, the viscosity of crude oil is an important physical property that influences and controls crude oil flow in pipelines. Viscosity introduces resistance to movement by causing a shear or frictional force between the fluid particles and the boundary walls. This high viscosity means that the pumping power requirements for crude oil in a long-distance pipeline are very high in order to overcome the increasing shear and friction forces. Therefore, in order to facilitate the pumping of these viscous oils and reduce operating expenses and the negative impact of pressure drops in pipelines during flow and processing, their viscosity must be reduced. Various techniques are used to increase pumping efficiency and improve the flow of crude oil through the pipeline, which may present logistical, technical or economic disadvantages for a given application. The main ones are the addition of surfactants or polymers, dilution with lighter crudes, use of water as annular fluid, thermal remediation and emulsification with surfactant (O/W). This review highlights the methods currently used to enhance the fluidity of heavy crude oil in pipelines behind rheology improvement, in particular the addition of additives and the use of water and surfactants to create a stable emulsion of heavy crude oil in water have been considered.
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    Experimental investigation of the rheological behavior of algerian crude oils from the quagmires
    (Taylor & Francis, 2019) Souas, Farid; Safri, Abdelhamid; Benmounah, Abdelbaki